Table 1
Data collection and refinement statistics
| NX1β-NL1 in citrate (Ca2+ chelated) | NX1β-NL1 adapted to acetate (Ca2+ un-chelated) | |
|---|---|---|
| Data collection | ||
| Space group | P212121 | P212121 |
| Cell dimensions | ||
| a, b, c (Å) | 116.59, 125.40, 131.86 | 120.62, 127.38, 133.26 |
| α, β, γ (°) | 90, 90, 90 | 90, 90, 90 |
| Resolution (Å) | 50-2.4(2.5-2.4)* | 50-3.5 (3.6-3.5) |
| Rmerge | 0.062 (0.463) | 0.067 (0.441) |
| I/σI | 19.3(3.2) | 18.4 (4.0) |
| Completeness (%) | 97.5(96.9) | 99.6 (99.7) |
| Redundancy | 4.5(4.0) | 5.1(5.4) |
| Refinement | ||
| Resolution (Å) | 50-2.4 | |
| No. reflections | 76375 | |
| Rwork / Rfree | 0.243 / 0.261 | |
| No. atoms | ||
| Protein | 11414 | |
| Ion | 2 | |
| Water | 1552 | |
| B-factors (Å2) | ||
| Protein | 61.1 | |
| Ion | 32.1 | |
| Water | 70.2 | |
| R.m.s. deviations | ||
| Bond length (Å) | 0.008 | |
| Bond angles (°) | 1.1 |
*One crystal was used for each dataset. Values in parentheses are for highest-resolution shell.